Self-assembly of nanoscopic coordination cages of D(3h) symmetry.

Kuehl, Christopher J; Kryschenko, Yury K; Radhakrishnan, Ukkirampandian; Seidel, S Russell; Huang, Songping D; Stang, Peter J · Proc Natl Acad Sci U S A · 2002

basic_science · Level V

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Abstract

A family of nanoscale-sized supramolecular cage compounds with a trigonal prismatic framework was prepared by means of spontaneous self-assembly from the combination of a predesigned molecular "clip" with tritopic pyridyl subunits. As confirmed by x-ray crystallography, the smallest structure of the reported series is approximately 1 x 2 nm and possesses a nitrate anion incarcerated inside its molecular cavity. The largest structure has dimensions of approximately 1 x 4 nm.

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