Orientational order in block copolymer films zone annealed below the order--disorder transition temperature.

Berry, Brian C; Bosse, August W; Douglas, Jack F; Jones, Ronald L; Karim, Alamgir · Nano Lett · 2007

basic_science · Level V

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Abstract

We report measurements of rapid ordering and preferential alignment in block copolymer films zone annealed below the order-disorder transition temperature. The orientational correlation lengths measured after approximately 5 h above the glass-transition temperature ( approximately 2 microm) were an order of magnitude greater than that obtained under equivalent static annealing. The ability to rapidly process polymers with inaccessible order-disorder transition temperatures suggests zone annealing as a route toward more robust nanomanufacturing methods based on block copolymer self-assembly.

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