Highly efficient NMR assignment of intrinsically disordered proteins: application to B- and T cell receptor domains.

Isaksson, Linnéa; Mayzel, Maxim; Saline, Maria; Pedersen, Anders; Rosenlöw, Joakim; Brutscher, Bernhard; Karlsson, B Göran; Orekhov, Vladislav Y · PLoS One · 2013

basic_science · Level V

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Abstract

We present an integrated approach for efficient characterization of intrinsically disordered proteins. Batch cell-free expression, fast data acquisition, automated analysis, and statistical validation with data resampling have been combined for achieving cost-effective protein expression, and rapid automated backbone assignment. The new methodology is applied for characterization of five cytosolic domains from T- and B-cell receptors in solution.

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