Deciphering the Elementary Steps of Transport-Reaction Processes at Individual Ag Nanoparticles by 3D Superlocalization Microscopy.

Patel, Anisha N; Martinez-Marrades, Ariadna; Brasiliense, Vitor; Koshelev, Dmitry; Besbes, Mondher; Kuszelewicz, Robert; Combellas, Catherine; Tessier, Gilles et al. · Nano Lett · 2015

basic_science · Level V

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Abstract

Transport-reaction processes at individual Ag nanoparticles (NPs) are studied using electrochemistry coupled with in situ 3D light scattering microscopy. Electrochemistry is used to trigger a (i) diffusiophoretic transport mode capable of accelerating and preconcentrating NPs toward an electrode and (ii) subsequent diffusion-controlled oxidation of NPs. Individual NP dissolution rate, analyzed using optical modeling, suggests the intervention of insoluble products. New insights into diverse NPs behaviors highlight the strength of coupled optical-electrochemical 3D microscopies for single-NP studies.