Thermally-induced reversible structural isomerization in colloidal semiconductor CdS magic-size clusters.

Zhang, Baowei; Zhu, Tingting; Ou, Mingyang; Rowell, Nelson; Fan, Hongsong; Han, Jiantao; Tan, Lei; Dove, Martin T et al. · Nat Commun · 2018

basic_science · Level V

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Abstract

Structural isomerism of colloidal semiconductor nanocrystals has been largely unexplored. Here, we report one pair of structural isomers identified for colloidal nanocrystals which exhibit thermally-induced reversible transformations behaving like molecular isomerization. The two isomers are CdS magic-size clusters with sharp absorption peaks at 311 and 322 nm. They have identical cluster masses, but slightly different structures. Furthermore, their interconversions follow first-order unimolecular reaction kinetics. We anticipate that such isomeric kinetics are applicable to a variety of small-size functional nanomaterials, and that the methodology developed for our kinetic study will be helpful to investigate and exploit solid-solid transformations in other semiconductor nanocrystals. The findings on structural isomerism should stimulate attention toward advanced design and synthesis of functional nanomaterials enabled by structural transformations.