Spin-phonon couplings in transition metal complexes with slow magnetic relaxation.

Moseley, Duncan H; Stavretis, Shelby E; Thirunavukkuarasu, Komalavalli; Ozerov, Mykhaylo; Cheng, Yongqiang; Daemen, Luke L; Ludwig, Jonathan; Lu, Zhengguang et al. · Nat Commun · 2018

basic_science · Level V

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Abstract

Spin-phonon coupling plays an important role in single-molecule magnets and molecular qubits. However, there have been few detailed studies of its nature. Here, we show for the first time distinct couplings of g phonons of Co<sup>II</sup>(acac)<sub>2</sub>(H<sub>2</sub>O)<sub>2</sub> (acac = acetylacetonate) and its deuterated analogs with zero-field-split, excited magnetic/spin levels (Kramers doublet (KD)) of the S = 3/2 electronic ground state. The couplings are observed as avoided crossings in magnetic-field-dependent Raman spectra with coupling constants of 1-2 cm<sup>-1</sup>. Far-IR spectra reveal the magnetic-dipole-allowed, inter-KD transition, shifting to higher energy with increasing field. Density functional theory calculations are used to rationalize energies and symmetries of the phonons. A vibronic coupling model, supported by electronic structure calculations, is proposed to rationalize the behavior of the coupled Raman peaks. This work spectroscopically reveals and quantitates the spin-phonon couplings in typical transition metal complexes and sheds light on the origin of the spin-phonon entanglement.