A highly reactive precursor in the iron sulfide system.

Matamoros-Veloza, Adriana; Cespedes, Oscar; Johnson, Benjamin R G; Stawski, Tomasz M; Terranova, Umberto; de Leeuw, Nora H; Benning, Liane G · Nat Commun · 2018

basic_science · Level V

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Abstract

Iron sulfur (Fe-S) phases have been implicated in the emergence of life on early Earth due to their catalytic role in the synthesis of prebiotic molecules. Similarly, Fe-S phases are currently of high interest in the development of green catalysts and energy storage. Here we report the synthesis and structure of a nanoparticulate phase (FeS<sub>nano</sub>) that is a necessary solid-phase precursor to the conventionally assumed initial precipitate in the iron sulfide system, mackinawite. The structure of FeS<sub>nano</sub> contains tetrahedral iron, which is compensated by monosulfide and polysulfide sulfur species. These together dramatically affect the stability and enhance the reactivity of FeS<sub>nano</sub>.

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