Exceptionally active iridium evolved from a pseudo-cubic perovskite for oxygen evolution in acid.

Chen, Yubo; Li, Haiyan; Wang, Jingxian; Du, Yonghua; Xi, Shibo; Sun, Yuanmiao; Sherburne, Matthew; Ager, Joel W et al. · Nat Commun · 2019

basic_science · Level V

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Abstract

Exploring robust catalysts for water oxidation in acidic electrolyte is challenging due to the limited material choice. Iridium (Ir) is the only active element with a high resistance to the acid corrosion during water electrolysis. However, Ir is rare, and its large-scale application could only be possible if the intrinsic activity of Ir could be greatly enhanced. Here, a pseudo-cubic SrCo<sub>0.9</sub>Ir<sub>0.1</sub>O<sub>3-δ</sub> perovskite, containing corner-shared IrO6 octahedrons, is designed. The Ir in the SrCo<sub>0.9</sub>Ir<sub>0.1</sub>O<sub>3-δ</sub> catalyst shows an extremely high intrinsic activity as reflected from its high turnover frequency, which is more than two orders of magnitude higher than that of IrO<sub>2</sub>. During the electrochemical cycling, a surface reconstruction, with Sr and Co leaching, over SrCo<sub>0.9</sub>Ir<sub>0.1</sub>O<sub>3-δ</sub> occurs. Such reconstructed surface region, likely contains a high amount of structural domains with corner-shared and under-coordinated IrO<sub>x</sub> octahedrons, is responsible for the observed high activity.