Carbon dioxide electroreduction to C<sub>2</sub> products over copper-cuprous oxide derived from electrosynthesized copper complex.

Zhu, Qinggong; Sun, Xiaofu; Yang, Dexin; Ma, Jun; Kang, Xinchen; Zheng, Lirong; Zhang, Jing; Wu, Zhonghua et al. · Nat Commun · 2019

basic_science · Level V

Where this comes from

Abstract

Efficient electroreduction of carbon dioxide to multicarbon products in aqueous solution is of great importance and challenging. Unfortunately, the low efficiency of the production of C<sub>2</sub> products limits implementation at scale. Here, we report reduction of carbon dioxide to C<sub>2</sub> products (acetic acid and ethanol) over a 3D dendritic copper-cuprous oxide composite fabricated by in situ reduction of an electrodeposited copper complex. In potassium chloride aqueous electrolyte, the applied potential was as low as -0.4 V vs reversible hydrogen electrode, the overpotential is only 0.53 V (for acetic acid) and 0.48 V (for ethanol) with high C<sub>2</sub> Faradaic efficiency of 80% and a current density of 11.5 mA cm<sup>-2</sup>. The outstanding performance of the electrode for producing the C<sub>2</sub> products results mainly from near zero contacting resistance between the electrocatalysts and copper substrate, abundant exposed active sites in the 3D dendritic structure and suitable copper(I)/copper(0) ratio of the electrocatalysts.