Dynamic oxygen adsorption on single-atomic Ruthenium catalyst with high performance for acidic oxygen evolution reaction.

Cao, Linlin; Luo, Qiquan; Chen, Jiajia; Wang, Lan; Lin, Yue; Wang, Huijuan; Liu, Xiaokang; Shen, Xinyi et al. · Nat Commun · 2019

basic_science · Level V

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Abstract

Achieving active and stable oxygen evolution reaction (OER) in acid media based on single-atom catalysts is highly promising for cost-effective and sustainable energy supply in proton electrolyte membrane electrolyzers. Here, we report an atomically dispersed Ru<sub>1</sub>-N<sub>4</sub> site anchored on nitrogen-carbon support (Ru-N-C) as an efficient and durable electrocatalyst for acidic OER. The single-atom Ru-N-C catalyst delivers an exceptionally intrinsic activity, reaching a mass activity as high as 3571 A g<sub>metal</sub><sup>-1</sup> and turnover frequency of 3348 O<sub>2</sub> h<sup>-1</sup> with a low overpotential of 267 mV at a current density of 10 mA cm<sup>-2</sup>. The catalyst shows no evident deactivation or decomposition after 30-hour operation in acidic environment. Operando synchrotron radiation X-ray absorption spectroscopy and infrared spectroscopy identify the dynamic adsorption of single oxygen atom on Ru site under working potentials, and theoretical calculations demonstrate that the O-Ru<sub>1</sub>-N<sub>4</sub> site is responsible for the high OER activity and stability.