Visualizing H<sub>2</sub>O molecules reacting at TiO<sub>2</sub> active sites with transmission electron microscopy.

Yuan, Wentao; Zhu, Beien; Li, Xiao-Yan; Hansen, Thomas W; Ou, Yang; Fang, Ke; Yang, Hangsheng; Zhang, Ze et al. · Science · 2020

basic_science · Level V

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Abstract

Imaging a reaction taking place at the molecular level could provide direct information for understanding the catalytic reaction mechanism. We used in situ environmental transmission electron microscopy and a nanocrystalline anatase titanium dioxide (001) surface with (1 × 4) reconstruction as a catalyst, which provided highly ordered four-coordinated titanium "active rows" to realize real-time monitoring of water molecules dissociating and reacting on the catalyst surface. The twin-protrusion configuration of adsorbed water was observed. During the water-gas shift reaction, dynamic changes in these structures were visualized on these active rows at the molecular level.