Single-pass transformation of syngas into ethanol with high selectivity by triple tandem catalysis.

Kang, Jincan; He, Shun; Zhou, Wei; Shen, Zheng; Li, Yangyang; Chen, Mingshu; Zhang, Qinghong; Wang, Ye · Nat Commun · 2020

basic_science · Level V

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Abstract

Synthesis of ethanol from non-petroleum carbon resources via syngas (a mixture of H<sub>2</sub> and CO) is an important but challenging research target. The current conversion of syngas to ethanol suffers from low selectivity or multiple processes with high energy consumption. Here, we report a high-selective conversion of syngas into ethanol by a triple tandem catalysis. An efficient trifunctional tandem system composed of potassium-modified ZnO-ZrO<sub>2</sub>, modified zeolite mordenite and Pt-Sn/SiC working compatibly in syngas stream in one reactor can afford ethanol with a selectivity of 90%. We demonstrate that the K<sup>+</sup>-ZnO-ZrO<sub>2</sub> catalyses syngas conversion to methanol and the mordenite with eight-membered ring channels functions for methanol carbonylation to acetic acid, which is then hydrogenated to ethanol over the Pt-Sn/SiC catalyst. The present work offers an effective methodology leading to high selective conversion by decoupling a single-catalyst-based complicated and uncontrollable reaction into well-controlled multi-steps in tandem in one reactor.