Tuning reactivity of Fischer-Tropsch synthesis by regulating TiO<sub>x</sub> overlayer over Ru/TiO<sub>2</sub> nanocatalysts.

Zhang, Yaru; Yang, Xiaoli; Yang, Xiaofeng; Duan, Hongmin; Qi, Haifeng; Su, Yang; Liang, Binglian; Tao, Huabing et al. · Nat Commun · 2020

basic_science · Level V

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Abstract

The activity of Fischer-Tropsch synthesis (FTS) on metal-based nanocatalysts can be greatly promoted by the support of reducible oxides, while the role of support remains elusive. Herein, by varying the reduction condition to regulate the TiO<sub>x</sub> overlayer on Ru nanocatalysts, the reactivity of Ru/TiO<sub>2</sub> nanocatalysts can be differentially modulated. The activity in FTS shows a volcano-like trend with increasing reduction temperature from 200 to 600 °C. Such a variation of activity is characterized to be related to the activation of CO on the TiO<sub>x</sub> overlayer at Ru/TiO<sub>2</sub> interfaces. Further theoretical calculations suggest that the formation of reduced TiO<sub>x</sub> occurs facilely on the Ru surface, and it involves in the catalytic mechanism of FTS to facilitate the CO bond cleavage kinetically. This study provides a deep insight on the mechanism of TiO<sub>x</sub> overlayer in FTS, and offers an effective approach to tuning catalytic reactivity of metal nanocatalysts on reducible oxides.