High-throughput gas separation by flexible metal-organic frameworks with fast gating and thermal management capabilities.

Hiraide, Shotaro; Sakanaka, Yuta; Kajiro, Hiroshi; Kawaguchi, Shogo; Miyahara, Minoru T; Tanaka, Hideki · Nat Commun · 2020

basic_science · Level V

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Abstract

Establishing new energy-saving systems for gas separation using porous materials is indispensable for ensuring a sustainable future. Herein, we show that ELM-11 ([Cu(BF<sub>4</sub>)<sub>2</sub>(4,4'-bipyridine)<sub>2</sub>]<sub>n</sub>), a member of flexible metal-organic frameworks (MOFs), exhibits rapid responsiveness to a gas feed and an 'intrinsic thermal management' capability originating from a structural deformation upon gas adsorption (gate-opening). These two characteristics are suitable for developing a pressure vacuum swing adsorption (PVSA) system with rapid operations. A combined experimental and theoretical study reveals that ELM-11 enables the high-throughput separation of CO<sub>2</sub> from a CO<sub>2</sub>/CH<sub>4</sub> gas mixture through adiabatic operations, which are extreme conditions in rapid pressure vacuum swing adsorption. We also propose an operational solution to the 'slipping-off' problem, which is that the flexible MOFs cannot adsorb target molecules when the partial pressure of the target gas decreases below the gate-opening pressure. Furthermore, the superiority of our proposed system over conventional systems is demonstrated.