In situ visualization of long-range defect interactions at the edge of melting.

Dresselhaus-Marais, Leora E; Winther, Grethe; Howard, Marylesa; Gonzalez, Arnulfo; Breckling, Sean R; Yildirim, Can; Cook, Philip K; Kutsal, Mustafacan et al. · Sci Adv · 2021

basic_science · Level V

Where this comes from

Abstract

Connecting a bulk material's microscopic defects to its macroscopic properties is an age-old problem in materials science. Long-range interactions between dislocations (line defects) are known to play a key role in how materials deform or melt, but we lack the tools to connect these dynamics to the macroscopic properties. We introduce time-resolved dark-field x-ray microscopy to directly visualize how dislocations move and interact over hundreds of micrometers deep inside bulk aluminum. With real-time movies, we reveal the thermally activated motion and interactions of dislocations that comprise a boundary and show how weakened binding forces destabilize the structure at 99% of the melting temperature. Connecting dynamics of the microstructure to its stability, we provide important opportunities to guide and validate multiscale models that are yet untested.