The active sites of Cu-ZnO catalysts for water gas shift and CO hydrogenation reactions.

Zhang, Zhenhua; Chen, Xuanye; Kang, Jincan; Yu, Zongyou; Tian, Jie; Gong, Zhongmiao; Jia, Aiping; You, Rui et al. · Nat Commun · 2021

basic_science · Level V

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Abstract

Cu-ZnO-Al<sub>2</sub>O<sub>3</sub> catalysts are used as the industrial catalysts for water gas shift (WGS) and CO hydrogenation to methanol reactions. Herein, via a comprehensive experimental and theoretical calculation study of a series of ZnO/Cu nanocrystals inverse catalysts with well-defined Cu structures, we report that the ZnO-Cu catalysts undergo Cu structure-dependent and reaction-sensitive in situ restructuring during WGS and CO hydrogenation reactions under typical reaction conditions, forming the active sites of Cu<sub>Cu(100)</sub>-hydroxylated ZnO ensemble and Cu<sub>Cu(611)</sub>Zn alloy, respectively. These results provide insights into the active sites of Cu-ZnO catalysts for the WGS and CO hydrogenation reactions and reveal the Cu structural effects, and offer the feasible guideline for optimizing the structures of Cu-ZnO-Al<sub>2</sub>O<sub>3</sub> catalysts.