A reasonable approach for the generation of hollow icosahedral kernels in metal nanoclusters.

Kang, Xi; Wei, Xiao; Liu, Xiaokang; Wang, Sicong; Yao, Tao; Wang, Shuxin; Zhu, Manzhou · Nat Commun · 2021

basic_science · Level V

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Abstract

Although the hollow icosahedral M<sub>12</sub> kernel has been extensively observed in metal nanoclusters, its origin remains a mystery. Here we report a reasonable avenue for the generation of the hollow icosahedron: the kernel collapse from several small nano-building blocks to an integrated hollow icosahedron. On the basis of the Au alloying processes from Ag<sub>28</sub>Cu<sub>12</sub>(SR)<sub>24</sub> to the template-maintained Au<sub>x</sub>Ag<sub>28-x</sub>Cu<sub>12</sub>(SR)<sub>24</sub> and then to the template-transformed Au<sub>12</sub>Cu<sub>y</sub>Ag<sub>32-y</sub>(SR)<sub>30</sub>, the kernel evolution/collapse from "tetrahedral Ag<sub>4</sub> + 4<sup>∗</sup>Ag<sub>3</sub>" to "tetrahedral Au<sub>4</sub> + 4<sup>∗</sup>M<sub>3</sub> (M = Au/Ag)" and then to "hollow icosahedral Au<sub>12</sub>" is mapped out. Significantly, the "kernel collapse" from small-sized nano-building blocks to large-sized nanostructures not only unveils the formation of hollow icosahedral M<sub>12</sub> in this work, but also might be a very common approach in constructing metallic kernels of nanoclusters and nanoparticles (not limited to the M<sub>12</sub> structure).