Unassisted selective solar hydrogen peroxide production by an oxidised buckypaper-integrated perovskite photocathode.

Mehrotra, Rashmi; Oh, Dongrak; Jang, Ji-Wook · Nat Commun · 2021

basic_science · Level V

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Abstract

Hydrogen peroxide (H<sub>2</sub>O<sub>2</sub>) is an eco-friendly oxidant and a promising energy source possessing comparable energy density to that of compressed H<sub>2</sub>. The current H<sub>2</sub>O<sub>2</sub> production strategies mostly depend on the anthraquinone oxidation process, which requires significant energy and numerous organic chemicals. Photocatalyst-based solar H<sub>2</sub>O<sub>2</sub> production comprises single-step O<sub>2</sub> reduction to H<sub>2</sub>O<sub>2</sub>, which is a simple and eco-friendly method. However, the solar-to-H<sub>2</sub>O<sub>2</sub> conversion efficiency is limited by the low performance of the inorganic semiconductor-based photoelectrodes and low selectivity and stability of the H<sub>2</sub>O<sub>2</sub> production electrocatalyst. Herein, we demonstrate unassisted solar H<sub>2</sub>O<sub>2</sub> production using an oxidised buckypaper as the H<sub>2</sub>O<sub>2</sub> electrocatalyst combined with a high-performance inorganic-organic hybrid (perovskite) photocathode, without the need for additional bias or sacrificial agents. This integrated photoelectrode system shows 100% selectivity toward H<sub>2</sub>O<sub>2</sub> and a solar-to-chemical conversion efficiency of ~1.463%.