A durable and pH-universal self-standing MoC-Mo<sub>2</sub>C heterojunction electrode for efficient hydrogen evolution reaction.

Liu, Wei; Wang, Xiting; Wang, Fan; Du, Kaifa; Zhang, Zhaofu; Guo, Yuzheng; Yin, Huayi; Wang, Dihua · Nat Commun · 2021

basic_science · Level V

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Abstract

Efficient water electrolyzers are constrained by the lack of low-cost and earth-abundant hydrogen evolution reaction (HER) catalysts that can operate at industry-level conditions and be prepared with a facile process. Here we report a self-standing MoC-Mo<sub>2</sub>C catalytic electrode prepared via a one-step electro-carbiding approach using CO<sub>2</sub> as the feedstock. The outstanding HER performances of the MoC-Mo<sub>2</sub>C electrode with low overpotentials at 500 mA cm<sup>-2</sup> in both acidic (256 mV) and alkaline electrolytes (292 mV), long-lasting lifetime of over 2400 h (100 d), and high-temperature performance (70 <sup>o</sup>C) are due to the self-standing hydrophilic porous surface, intrinsic mechanical strength and self-grown MoC (001)-Mo<sub>2</sub>C (101) heterojunctions that have a ΔG<sub>H*</sub> value of -0.13 eV in acidic condition, and the energy barrier of 1.15 eV for water dissociation in alkaline solution. The preparation of a large electrode (3 cm × 11.5 cm) demonstrates the possibility of scaling up this process to prepare various carbide electrodes with rationally designed structures, tunable compositions, and favorable properties.