Thermally boosted upconversion and downshifting luminescence in Sc<sub>2</sub>(MoO<sub>4</sub>)<sub>3</sub>:Yb/Er with two-dimensional negative thermal expansion.

Liao, Jinsheng; Wang, Minghua; Lin, Fulin; Han, Zhuo; Fu, Biao; Tu, Datao; Chen, Xueyuan; Qiu, Bao et al. · Nat Commun · 2022

basic_science · Level V

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Abstract

Rare earth (RE<sup>3+</sup>)-doped phosphors generally suffer from thermal quenching, in which their photoluminescence (PL) intensities decrease at high temperatures. Herein, we report a class of unique two-dimensional negative-thermal-expansion phosphor of Sc<sub>2</sub>(MoO<sub>4</sub>)<sub>3</sub>:Yb/Er. By virtue of the reduced distances between sensitizers and emitters as well as confined energy migration with increasing the temperature, a 45-fold enhancement of green upconversion (UC) luminescence and a 450-fold enhancement of near-infrared downshifting (DS) luminescence of Er<sup>3+</sup> are achieved upon raising the temperature from 298 to 773 K. The thermally boosted UC and DS luminescence mechanism is systematically investigated through in situ temperature-dependent Raman spectroscopy, synchrotron X-ray diffraction and PL dynamics. Moreover, the luminescence lifetime of <sup>4</sup>I<sub>13/2</sub> of Er<sup>3+</sup> in Sc<sub>2</sub>(MoO<sub>4</sub>)<sub>3</sub>:Yb/Er displays a strong temperature dependence, enabling luminescence thermometry with the highest relative sensitivity of 12.3%/K at 298 K and low temperature uncertainty of 0.11 K at 623 K. These findings may gain a vital insight into the design of negative-thermal-expansion RE<sup>3+</sup>-doped phosphors for versatile applications.