Unlocking bimetallic active sites via a desalination strategy for photocatalytic reduction of atmospheric carbon dioxide.

Feng, Xuezhen; Zheng, Renji; Gao, Caiyan; Wei, Wenfei; Peng, Jiangguli; Wang, Ranhao; Yang, Songhe; Zou, Wensong et al. · Nat Commun · 2022

basic_science · Level V

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Abstract

Ultrathin two-dimensional (2D) metal oxyhalides exhibit outstanding photocatalytic properties with unique electronic and interfacial structures. Compared with monometallic oxyhalides, bimetallic oxyhalides are less explored. In this work, we have developed a novel top-down wet-chemistry desalination approach to remove the alkali-halide salt layer within the complicated precursor bulk structural matrix Pb<sub>0.6</sub>Bi<sub>1.4</sub>Cs<sub>0.6</sub>O<sub>2</sub>Cl<sub>2</sub>, and successfully fabricate a new 2D ultrathin bimetallic oxyhalide Pb<sub>0.6</sub>Bi<sub>1.4</sub>O<sub>2</sub>Cl<sub>1.4</sub>. The unlocked larger surface area, rich bimetallic active sites, and faster carrier dynamics within Pb<sub>0.6</sub>Bi<sub>1.4</sub>O<sub>2</sub>Cl<sub>1.4</sub> layers significantly enhance the photocatalytic efficiency for atmospheric CO<sub>2</sub> reduction. It outperforms the corresponding parental matrix phase and other state-of-the-art bismuth-based monometallic oxyhalides photocatalysts. This work reports a top-down desalination strategy to engineering ultrathin bimetallic 2D material for photocatalytic atmospheric CO<sub>2</sub> reduction, which sheds light on further constructing other ultrathin 2D catalysts for environmental and energy applications from similar complicate structure matrixes.