Strain in Copper/Ceria Heterostructure Promotes Electrosynthesis of Multicarbon Products.

Wang, Haibin; Zhang, Hao; Huang, Yan; Wang, Haiyu; Ozden, Adnan; Yao, Kaili; Li, Huamin; Guo, Qianying et al. · ACS Nano · 2023

basic_science · Level V

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Abstract

Elastic strains in metallic catalysts induce enhanced selectivity for carbon dioxide reduction (CO<sub>2</sub>R) toward valuable multicarbon (C<sub>2+</sub>) products. However, under working conditions, the structure of catalysts inevitably undergoes reconstruction, hardly retaining the initial strain. Herein, we present a metal/metal oxide synthetic strategy to introduce and maintain the tensile strain in a copper/ceria heterostructure, enabled by the presence of a thin interface layer of Cu<sub>2</sub>O/CeO<sub>2</sub>. The tensile strain in the copper domain and deficient electron environment around interfacial Cu sites resulted in strengthened adsorption of carbonaceous intermediates and promoted *CO dimerization. The strain effect in the copper/ceria heterostructure leads to an improved C<sub>2+</sub> selectivity with a maximum Faradaic efficiency of 76.4% and a half-cell power conversion efficiency of 49.1%. The fundamental insights gained from this system can facilitate the rational design of heterostructure catalysts for CO<sub>2</sub>R.