Active and durable R<sub>2</sub>MnRuO<sub>7</sub> pyrochlores with low Ru content for acidic oxygen evolution.

Galyamin, Dmitry; Torrero, Jorge; Rodríguez, Isabel; Kolb, Manuel J; Ferrer, Pilar; Pascual, Laura; Salam, Mohamed Abdel; Gianolio, Diego et al. · Nat Commun · 2023

basic_science · Level V

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Abstract

The production of green hydrogen in water electrolyzers is limited by the oxygen evolution reaction (OER). State-of-the-art electrocatalysts are based on Ir. Ru electrocatalysts are a suitable alternative provided their performance is improved. Here we show that low-Ru-content pyrochlores (R<sub>2</sub>MnRuO<sub>7</sub>, R = Y, Tb and Dy) display high activity and durability for the OER in acidic media. Y<sub>2</sub>MnRuO<sub>7</sub> is the most stable catalyst, displaying 1.5 V at 10 mA cm<sup>-2</sup> for 40 h, or 5000 cycles up to 1.7 V. Computational and experimental results show that the high performance is owed to Ru sites embedded in RuMnO<sub>x</sub> surface layers. A water electrolyser with Y<sub>2</sub>MnRuO<sub>7</sub> (with only 0.2 mg<sub>Ru</sub> cm<sup>-2</sup>) reaches 1 A cm<sup>-2</sup> at 1.75 V, remaining stable at 200 mA cm<sup>-2</sup> for more than 24 h. These results encourage further investigation on Ru catalysts in which a partial replacement of Ru by inexpensive cations can enhance the OER performance.