Evolution of dislocation substructures in metals via high-strain-rate nanoindentation.

Zhang, Yuwei; Hackett, Benjamin L; Dong, Jiaqi; Xie, Kelvin Y; Pharr, George M · Proc Natl Acad Sci U S A · 2023

biomechanical · Level V

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Abstract

Deformation at high strain rates often results in high stresses on many engineering materials, potentially leading to catastrophic failure without proper design. High-strain-rate mechanical testing is thus needed to improve the design of future structural materials for a wide range of applications. Although several high-strain-rate mechanical testing techniques have been developed to provide a fundamental understanding of material responses and microstructural evolution under high-strain-rate deformation conditions, these tests are often very time consuming and costly. In this work, we utilize a high-strain-rate nanoindentation testing technique and system in combination with transmission electron microscopy to reveal the deformation mechanisms and dislocation substructures that evolve in pure metals from low (10<sup>-2</sup> s<sup>-1</sup>) to very high indentation strain rates (10<sup>4</sup> s<sup>-1</sup>), using face-centered cubic aluminum and body-centered cubic molybdenum as model materials. The results help to establish the conditions under which micro- and macro-scale tests can be compared with validity and also provide a promising pathway that could lead to accelerated high-strain-rate testing at substantially reduced costs.