Spontaneous Supercrystal Formation During a Strain-Engineered Metal-Insulator Transition.

Gorobtsov, Oleg Yu; Miao, Ludi; Shao, Ziming; Tan, Yueze; Schnitzer, Noah; Goodge, Berit Hansen; Ruf, Jacob; Weinstock, Daniel et al. · Adv Mater · 2024

basic_science · Level V

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Abstract

Mott metal-insulator transitions possess electronic, magnetic, and structural degrees of freedom promising next-generation energy-efficient electronics. A previously unknown, hierarchically ordered, and anisotropic supercrystal state is reported and its intrinsic formation characterized in-situ during a Mott transition in a Ca<sub>2</sub>RuO<sub>4</sub> thin film. Machine learning-assisted X-ray nanodiffraction together with cryogenic electron microscopy reveal multi-scale periodic domain formation at and below the film transition temperature (T<sub>Film</sub> ≈ 200-250 K) and a separate anisotropic spatial structure at and above T<sub>Film</sub>. Local resistivity measurements imply an intrinsic coupling of the supercrystal orientation to the material's anisotropic conductivity. These findings add a new degree of complexity to the physical understanding of Mott transitions, opening opportunities for designing materials with tunable electronic properties.