Phosphorus Oxidation Controls Epitaxial Shell Growth in InP/ZnSe Quantum Dots.

Ubbink, Reinout F; Speelman, Tom; Esteban, Daniel Arenas; van Leeuwen, Mourijn; Stam, Maarten; Bals, Sara; De Wijs, Gilles A; van Eck, Ernst R H et al. · ACS Nano · 2025

basic_science · Level V

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Abstract

InP/ZnSe/ZnS core/shell/shell quantum dots are the most investigated quantum dot material for commercial applications involving visible light emission. The inner InP/ZnSe interface is complex since it is not charge balanced, and the InP surface is prone to oxidation. The role of oxidative defects at this interface has remained a topic of debate, with conflicting reports of both detrimental and beneficial effects on the quantum dot properties. In this study we probe the structure of the InP/ZnSe interface at the atomic level using <sup>31</sup>P, <sup>77</sup>Se and <sup>17</sup>O ssNMR and HAADF-STEM. We observe clear differences in Se NMR spectra and crystal orientation of core and shell when the InP/ZnSe is oxidized on purpose. High levels of interface oxidation result in an amorphous phosphate layer at the interface, which inhibits epitaxial growth of the ZnSe shell.