Antiferrodistortive and Ferroeletric Phase Transitions in Freestanding Films of SrTiO<sub>3</sub>.

Leroy, Ludmila; Huang, Shih-Wen; Chiu, Chun-Chien; Ho, Sheng-Zhu; Dössegger, Janine; Piamonteze, Cinthia; Chen, Yi-Chun; Abreu, Elsa et al. · Nano Lett · 2025

basic_science · Level V

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Abstract

Thin films' properties can be greatly influenced by their supporting growth substrates. Even in the so-called strain-free heterostructure films, it is still unclear whether there will be no interfacial electronic reconstructions induced by the underlying substrates. Here, we report the studies of SrTiO<sub>3</sub> (STO) films in the freestanding form (FS) with a thickness ranging from 20 to 80 nm. These STO films, by default, are in a strain-free state; they exhibit distinct properties not seen in both bulk and strain-free heterostructure forms. Our films show an enhanced antiferrodistortive (AFD) phase transition temperature with a preferential in-plane rotation axis for the TiO<sub>6</sub> octahedra. The anisotropic Ti orbital occupancy around the surface signals the departure of its properties from the bulk. Moreover, we have found that the in-plane ferroelectricity can be strengthened by the reduced dimensionality, establishing that the dimensionality control is an important factor for enhancing STO's ferroelectric response.