Tunable-Diameter Nanoscrolls from Janus WSSe/WSe<sub>2</sub> Heterostructures.

Kaneda, Masahiko; Zhang, Wenjin; Bi, Dingkun; Sun, Tianyishan; Ogura, Hiroto; Endo, Takahiko; Takahashi, Yuta; Fujii, Shun et al. · ACS Nano · 2025

basic_science · Level V

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Abstract

Janus transition metal dichalcogenide (TMD) nanoscrolls have recently emerged as promising nanostructures for studying curvature- and chirality-dependent physical phenomena. However, systematic strategies to fabricate multilayer Janus TMD nanoscrolls with controlled diameters and to probe their structure-dependent optical behaviors are still lacking. Expanding on the previous finding that Janus TMD monolayers─with intrinsic asymmetry and built-in strain─spontaneously form nanoscrolls, we now demonstrate diameter-tunable nanoscrolls derived from Janus WSSe/WSe<sub>2</sub> heterostructures. The incorporation of a Janus monolayer facilitates the scrolling of heterostructures and enables continuous tuning of nanoscroll diameters across a broad range─from ∼10 nm to ∼1 μm. The resulting structures exhibit uniform crystallinity and composition, as confirmed by scanning transmission electron microscopy. Optical characterizations reveal anisotropic Raman responses and strain-induced modulation of second-harmonic generation (SHG). These results indicate that Janus-based nanoscrolls provide a versatile platform for investigating structure-property relationships and developing rolled TMD systems for advanced photonic and optoelectronic applications.