Metallic Lead Formation in Perovskites: Mechanisms, Suppression, and Future Directions.

Abdelhady, Ahmed L; Afraj, Shakil N; Haruta, Yuki; Uddin, Mohammed Misbah; Saidaminov, Makhsud I · ACS Nano · 2025

review · Level V

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Abstract

Lead halide perovskites APbX<sub>3</sub> (A = methylammonium, formamidinium, cesium; X = halogen) have advanced the field of optoelectronics, particularly in solar cells, photodetectors, and light-emitting diodes, due to their outstanding properties. However, a significant challenge remains unresolved: the formation of metallic lead (Pb<sup>0</sup>), which introduces deep-level defects that trap charge carriers and degrade device performance. The formation of Pb<sup>0</sup> in perovskites can occur after their synthesis under various conditions, including high-energy radiation, light, heat, and moisture, and has also been observed during perovskite crystallization. Thus, it is crucial to understand the underlying mechanisms of Pb<sup>0</sup> formation and its suppression pathways. Recent studies have explored various strategies to suppress Pb<sup>0</sup> formation, including compositional engineering, additive incorporation, and protective passivation layers. In this review, we discuss the origins of Pb<sup>0</sup> formation in perovskites, focusing on the mechanisms driving this process under different environmental conditions, and then strategies for suppressing Pb<sup>0</sup> formation, including compositional engineering and passivation techniques. By addressing these aspects, we seek to identify pathways for enhancing the stability and performance of perovskite-based devices, enabling their widespread adoption in commercial applications.