Continuous flow photosynthesis of methanol from methane by plasmonic charge accumulation.

Peng, Huiping; Xue, Fei; Ji, Yujin; Li, Youyong; Liu, Shangheng; Kong, Qingyu; Hu, Zhiwei; Zheng, Xuanli et al. · Nat Commun · 2025

basic_science · Level V

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Abstract

Direct oxidation of methane (CH<sub>4</sub>) to methanol (CH<sub>3</sub>OH) typically requires elevated temperatures and pressures, making it challenging to achieve high yield and selectivity under mild conditions. Here, we show a surface plasmon-mediated catalyst designing strategy based on the synergy between Pd nanoparticles and ZnO nanosheets. When applied in a continuous gas-solid-liquid photocatalytic flow system at low temperature and ambient pressure, the optimized catalyst achieves a CH<sub>3</sub>OH productivity of 6584 μmol g<sup>-1</sup> h<sup>-1</sup>, which is competitive with reported photocatalytic systems, along with selectivity of ~100% and sustained stability over 100 h. In-situ characterization and theoretical calculations indicate that plasmon-induced electron accumulation suppresses over-oxidation and promotes high CH<sub>3</sub>OH selectivity. This work offers a pathway to efficient, selective CH<sub>4</sub> photo-oxidation using plasmonic catalyst design, supporting the sustainable utilization of solar energy.