Co-modulating CO Adsorption and Interfacial Water Dissociation through a Lewis Acid Site Boosts Industrial CO<sub>2</sub>-to-Ethylene Conversion.

Wei, Changze; Lin, Zheng; Han, Guokang; Qian, Zhengyi; Zhao, Yilin; Liu, Fei; Tan, Yingjun; Ye, Na et al. · Nano Lett · 2026

basic_science · Level V

Where this comes from

Abstract

Copper-based electrocatalysts have shown great potential for electrolytic CO<sub>2</sub> reduction (CO<sub>2</sub>RR) to value-added multi-carbon products but suffer from poor selectivity and activity due to the uncontrollable CO adsorption and sluggish C-C coupling kinetics. Herein, we develop a dopant-driven interfacial engineering strategy by incorporating chromium (Cr) into copper oxide, which <i>in situ</i> reconstructs to Cu-CrO<sub><i>x</i></sub> heterointerfaces under CO<sub>2</sub>RR conditions. Combined experimental and theoretical analyses reveal that Lewis acidic CrO<i><sub>x</sub></i> clusters tailor the electronic structure of Cu sites, thereby strengthening the CO adsorption and accelerating C-C coupling. The Cu-CrO<i><sub>x</sub></i> interface also promotes water dissociation to supply active hydrogen species for multiple hydrogenation steps. The optimized catalyst achieves a 59.2% faradaic efficiency for ethylene and maintains stable operation for over 110 h at 2.45 V in a membrane electrode assembly electrolyzer. This work highlights dopant-enabled interfacial engineering as a versatile strategy for steering CO<sub>2</sub>RR activity and selectivity toward multi-carbon products, offering mechanistic insights that advance the field.